Triphenylamine → HCID 86760631, compound

HRID 1393612Notes

Reaction equation

HRID 1393612 reaction equation
[CH3:1][OH:2].[C:3]1([N:9]([C:16]2[CH:21]=[CH:20][CH:19]=[CH:18][CH:17]=2)[C:10]2[CH:15]=[CH:14][CH:13]=[CH:12][CH:11]=2)[CH:8]=[CH:7][CH:6]=[CH:5][CH:4]=1.C1(N(C2C=CC=CC=2)C2C=CC=CC=2)C=CC=CC=1.[C:41](Cl)(=[O:44])[CH:42]=[CH2:43]>C1C=CC=CC=1>[CH3:1][O:2][C:41](=[O:44])[CH:42]=[CH2:43].[C:16]1([N:9]([C:3]2[CH:4]=[CH:5][CH:6]=[CH:7][CH:8]=2)[C:10]2[CH:15]=[CH:14][CH:13]=[CH:12][CH:11]=2)[CH:17]=[CH:18][CH:19]=[CH:20][CH:21]=1

Participants

5

Reactant 3

HCID 11775TriphenylamineHCID 13140Acryloyl chloride2×HCID 18326016HCID 18326016, compound2×

Product 1

HCID 86760631HCID 86760631, compound

Reagents, catalysts & solvents 1

HCID 241BenzeneSolvent2×

Procedure

(Procedure 1): Triphenylamine methyl alcohol as a triphenylamine derivative and an acrylic acid chloride were dissolved in benzene, and then the resultant benzene solution was stirred at 0° C. for five hours so as to cause the triphenylamine methyl alcohol to react with the acrylic acid chloride. After the reaction, the benzene solution was evaporated under reduced pressure so as to obtain a triphenylamine methyl acrylate monomer as a crude crystal. Next, the crude crystal was recrystallized by benzene for purification. The reaction scheme of the triphenylamine methyl alcohol and the acrylic acid chloride is shown in Scheme 1.

Workup

  1. customAfter the reaction
  2. customthe benzene solution was evaporated under reduced pressure so as

Sources & evidence

ORD record
ord-7340d0b6e0ed476f99904bfad84649bd
Source dataset
uspto-grants-2008_03
Patent number
US07345141B2

Reaction notes

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