HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triphenylamine → HCID 86760631, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triphenylamine | HCID 11775 | — |
| Reactant | Acryloyl chloride | HCID 13140 | — |
| Reactant | HCID 18326016 | HCID 18326016 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | HCID 86760631 | HCID 86760631 | — |
Reaction Steps
(Procedure 1): Triphenylamine methyl alcohol as a triphenylamine derivative and an acrylic acid chloride were dissolved in benzene, and then the resultant benzene solution was stirred at 0° C. for five hours so as to cause the triphenylamine methyl alcohol to react with the acrylic acid chloride. After the reaction, the benzene solution was evaporated under reduced pressure so as to obtain a triphenylamine methyl acrylate monomer as a crude crystal. Next, the crude crystal was recrystallized by benzene for purification. The reaction scheme of the triphenylamine methyl alcohol and the acrylic acid chloride is shown in Scheme 1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07345141B2 |
| Source dataset | uspto-grants-2008_03 |
| ORD ID | ord-7340d0b6e0ed476f99904bfad84649bd |
| Source note | uspto-grants-2008_03 |