HRID1393834

反应详情

EQUATION

反应方程式

HRID 1393834 反应方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

1 g of 2-(4-nitrophenylamino)ethanesulfonamide (12) was suspended in 10 mL of ethanol. At room temperature, the suspension was poured onto a reductive solution of sodium hydrosulfite (8 g)—1N sodium hydroxide (30 mL). After decolorization, a precipitate formed. 0.7 g of crude product was isolated by suction-filtering and reslurrying in water.

WORKUP

后处理

  1. customAfter decolorization, a precipitate formed