HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Dithionite → 2-(4-Aminophenylamino)ethanesulfonamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Dithionite | HCID 24489 | — |
| Reactant | 2-(4-Nitrophenylamino)ethanesulfonamide | HCID 23104441 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 2-(4-Aminophenylamino)ethanesulfonamide | HCID 23104443 | 79.7% |
Reaction Steps
1 g of 2-(4-nitrophenylamino)ethanesulfonamide (12) was suspended in 10 mL of ethanol. At room temperature, the suspension was poured onto a reductive solution of sodium hydrosulfite (8 g)—1N sodium hydroxide (30 mL). After decolorization, a precipitate formed. 0.7 g of crude product was isolated by suction-filtering and reslurrying in water.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07347879B2 |
| Source dataset | uspto-grants-2008_03 |
| ORD ID | ord-2535bde458e24411a61dd72c00e52b04 |
| Source note | uspto-grants-2008_03 |