HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 86599745, compound → HCID 86599744, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 86599745 | HCID 86599745 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 86599744 | HCID 86599744 | — |
Reaction Steps
Palladium black (52 mg) was added to a solution of (3S)-3-benzyloxycarbonylamino-1-bis(methylamino)phosphinyl-2-piperidone (524.1 mg, 1.4791 mmol) in methanol (5.2 mL), and the resulting mixture was stirred at room temperature for 3 hours under a hydrogen atmosphere.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07348318B2 |
| Source dataset | uspto-grants-2008_03 |
| ORD ID | ord-1eeb1a7165f1463892f5331efd812c3c |
| Source note | uspto-grants-2008_03 |