HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 178458089, compound → HCID 178458088, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 178458089 | HCID 178458089 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 178458088 | HCID 178458088 | — |
Reaction Steps
Palladium black (16 mg) was added to a solution of (3S)-3-benzyloxycarbonylamino-1-amino(n-propylamino)phosphinyl-2-piperidone (161.1 g, 0.4373 mmol) in methanol (3 mL), and the resulting mixture was stirred at room temperature for 50 minutes under a hydrogen atmosphere.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07348318B2 |
| Source dataset | uspto-grants-2008_03 |
| ORD ID | ord-c44e1675fede41c9991429b04438c544 |
| Source note | uspto-grants-2008_03 |