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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1393953Generated: November 3, 2026

Methyl iodide → HCID 178503334, compound

https://huagongshe.com/reaction/1393953

Reaction equation

Participants

RoleNameHCIDCharge
ReactantMethyl iodideHCID 6328—
ReactantHCID 12360758HCID 12360758—
SolventAcetoneHCID 180—
ProductHCID 178503334HCID 17850333467.9%

Reaction Steps

Methyl iodide (0.43 ml, 6.94 mmol) was added to a solution of 4-methyl-3,4-dihydro-1H-quinazoline-2-thione (410 mg, 2.30 mmol) in acetone (5 ml). The mixture was stirred for 15 min (r.t.), and the title compound (500 mg, 67%) was isolated from the reaction mixture by filtration.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07348332B2
Source datasetuspto-grants-2008_03
ORD IDord-8d565d8b9680445abbe8b27ed2e0f16b
Source noteuspto-grants-2008_03