HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → HCID 178503334, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | HCID 12360758 | HCID 12360758 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 178503334 | HCID 178503334 | 67.9% |
Reaction Steps
Methyl iodide (0.43 ml, 6.94 mmol) was added to a solution of 4-methyl-3,4-dihydro-1H-quinazoline-2-thione (410 mg, 2.30 mmol) in acetone (5 ml). The mixture was stirred for 15 min (r.t.), and the title compound (500 mg, 67%) was isolated from the reaction mixture by filtration.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07348332B2 |
| Source dataset | uspto-grants-2008_03 |
| ORD ID | ord-8d565d8b9680445abbe8b27ed2e0f16b |
| Source note | uspto-grants-2008_03 |