HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 13839927, compound → HCID 16109184, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 13839927 | HCID 13839927 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 16109184 | HCID 16109184 | 68% |
Reaction Steps
The title compound (1.2 g, 68%) was prepared from ethyl 2-methyl-2-(4-nitrophenyloxy)propanoate (2 g, 7.9 mmol) by hydrogenation with 10% Pd/C (1 g) in methanol at 50 psi and room temperature for 2 h.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07348334B2 |
| Source dataset | uspto-grants-2008_03 |
| ORD ID | ord-811ce096333a446d89af0110909a2d28 |
| Source note | uspto-grants-2008_03 |