HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Acid → HCID 59681882, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | Piperidine | HCID 8082 | — |
| Reactant | Oxazolidine-2,5-dione | HCID 75136 | — |
| Reactant | 4-(4-Fluorophenoxy)benzaldehyde | HCID 3856802 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 59681882 | HCID 59681882 | — |
Reaction Steps
The title compound was prepared by reacting 4-(4-fluorophenoxy)benzaldehyde (from Step A in Example 1) with oxazolidine-2,5-dione in toluene in the presence of piperidine and acetic acid with continuous removal of water, as described in Step B of Example 1. The crystalline product collected was washed with petroleum ether on the filter and dried in vacuo.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07348348B2 |
| Source dataset | uspto-grants-2008_03 |
| ORD ID | ord-ab0c74f6c3ca4698b2b17f6384e78c7e |
| Source note | uspto-grants-2008_03 |