HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → HCID 69158965, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 69159360 | HCID 69159360 | — |
| Solvent | Hydrochloric Acid | HCID 313 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 69158965 | HCID 69158965 | — |
Reaction Steps
The product from Step 1 (0.245 g, 0.64 mmole) in 1,4-dioxane (20 ml) and aqueous hydrochloric acid (5M, 10 ml) was heated under reflux for 18 hours. The mixture was allowed to cool to ambient temperature, neutralised by addition of aqueous sodium hydroxide solution (5M) and extracted into dichloromethane.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07348339B2 |
| Source dataset | uspto-grants-2008_03 |
| ORD ID | ord-cdd082d6d0884e4fac6ade4a4c320331 |
| Source note | uspto-grants-2008_03 |