HuagongsheHuagongshe Chemistry Print Report · For research reference only
Oxalyl chloride → HCID 17981884, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Oxalyl chloride | HCID 65578 | — |
| Reactant | HCID 17981886 | HCID 17981886 | — |
| Catalyst | Dimethylformamide | HCID 6228 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 17981884 | HCID 17981884 | — |
Reaction Steps
To a solution of acid from step 4 in CH2Cl2 (0.2M) was added oxalyl chloride (1.2 eq) and one drop of DMF. The mixture was stirred at rt for 3 h and the solvent evaporated. The crude acid chloride was used as such in the next step.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07348433B2 |
| Source dataset | uspto-grants-2008_03 |
| ORD ID | ord-0654e37ea4f84859a51ca05c4242cdc5 |
| Source note | uspto-grants-2008_03 |