HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phosphorus oxychloride → 4-Chloromethyl-2-(4-fluoro-3-methyl-phenyl)-5-methyl-oxazole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phosphorus oxychloride | HCID 24813 | — |
| Reactant | HCID 22273855 | HCID 22273855 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | 4-Chloromethyl-2-(4-fluoro-3-methyl-phenyl)-5-methyl-oxazole | HCID 21974259 | — |
Reaction Steps
In analogy to the procedure described in example 2 b], 2-(4-fluoro-3-methyl-phenyl)-4,5-dimethyl-oxazole 3-oxide was treated with phosphorous oxychloride in chloroform to yield 4-chloromethyl-2-(4-fluoro-3-methyl-phenyl)-5-methyl-oxazole as colorless solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07348349B2 |
| Source dataset | uspto-grants-2008_03 |
| ORD ID | ord-94f55a9be3b54526847e02aa35c642c0 |
| Source note | uspto-grants-2008_03 |