HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Quinolinecarboxylic acid → Quinoline-4-carbonyl chloride hydrochloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Quinolinecarboxylic acid | HCID 10243 | — |
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Product | Quinoline-4-carbonyl chloride hydrochloride | HCID 12373997 | 78% |
Reaction Steps
2-[4'-(5"-nitrofuryl-2")-1,3-butadienyl]quinoline-4-carboxylic acid chloride hydrochloride was prepared as described in Example 1 from 2-[4-(5"-nitrofuryl-2")-1,3-butadienyl]quinoline-4-carboxylic acid and thionyl chloride with the yield of 78%, m.p. 230°-232° C. (with decomposition).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04201784 |
| Source dataset | uspto-grants-1980_05 |
| ORD ID | ord-1c6ffbfba08d4293ad89afe78044feb5 |
| Source note | uspto-grants-1980_05 |