HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phosphoric Acid → Quinoline-4-carboxylic acid (alpha-methyl-delta-diethylaminobutyl)amide diphosphate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phosphoric Acid | HCID 1004 | — |
| Reactant | Quinoline-4-carboxylic acid (alpha-methyl-delta-diethylaminobutyl)amide | HCID 86736974 | — |
| Product | Quinoline-4-carboxylic acid (alpha-methyl-delta-diethylaminobutyl)amide diphosphate | HCID 86736975 | 68.1% |
Reaction Steps
2-[4'-(5"-nitrofuryl-2")-1,3-butadienyl]quinoline-4-carboxylic acid (α-methyl-δ-diethylaminobutyl)amide diphosphate was prepared as described in Example 9 from 2-[2'-(5"-nitrofuryl-2")vinyl]quinoline-4-carboxylic acid (α-methyl-δ-diethylaminobutyl)amide and ortho-phosphoric acid. The yield was 68.1%, m.p. 176°-178° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04201784 |
| Source dataset | uspto-grants-1980_05 |
| ORD ID | ord-dd75330445c74dcab98750422aaea439 |
| Source note | uspto-grants-1980_05 |