Hydrochloric Acid → HCID 20340251, compound

Participants

Reaction Steps

10 G. of 4-{[[3-(p-chlorophenyl)propyl]thiocarbamoyl]-thio}-butyric acid ethyl ester dissolved in 100 ml. of acetic acid were stirred under slight reflux for 8 hours with 50 ml. of half-concentrated hydrochloric acid. The mixture was evaporated in vacuo, the residue recrystallized from carbon tetrachloride, and 4.4 g. of 4-{[[(p-chlorophenyl)propyl]-thiocarbamoyl]thio}-butyric acid having a melting point of 98°-100° C. were obtained.

Provenance & Evidence