HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diazomethane → HCID 54488354, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diazomethane | HCID 9550 | — |
| Reactant | 4-({[(4-Chlorophenyl)methyl]carbamothioyl}sulfanyl)butanoic acid | HCID 20340272 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 54488354 | HCID 54488354 | — |
Reaction Steps
1.5 G. of 4-{[(p-chlorobenzyl)thiocarbamoyl]thio}-butyric acid were dissolved in 30 ml. of diethyl ether and treated with an excess of an ethereal diazomethane solution. The resulting solution was evaporated. The residue was recrystallized from cyclohexane, and 1.2 g. of 4-{[(p-chlorobenzyl)thiocarbamoyl]thio}-butyric acid methyl ester having a melting point of 60°-62° C. were obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04202832 |
| Source dataset | uspto-grants-1980_05 |
| ORD ID | ord-eff9508acb444f87b1c47e2088508cdd |
| Source note | uspto-grants-1980_05 |