Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Methane | HCID 297 | — |
| Reactant | Allyl glycidyl ether | HCID 7838 | — |
| Reactant | HCID 19020936 | HCID 19020936 | — |
| Catalyst | Tetramethylammonium chloride | HCID 6379 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 20340333 | HCID 20340333 | — |
Reaction Steps
Into a round bottom flask was charged 29 g. (0.1 moles) of 2-hydroxyethyl 2-cyano-3,3-diphenylacrylate, 12.4 g. (0.11 moles) of allyl glycidyl ether and 250 mg. of tetramethylammonium chloride. The flask was stoppered and the mixture was heated at 50° C. for 16 hours. Then cooled mixture was diluted with 50 ml. methylene dichloride, treated with decolonizing charcoal and filtered. The filtrate was evaporated, leaving a pale yellow oil characterized as the product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04202834 |
|---|
| Source dataset | uspto-grants-1980_05 |
|---|
| ORD ID | ord-ff1372e138e041d8a8cbd4a6dadb0c43 |
|---|
| Source note | uspto-grants-1980_05 |
|---|
