Trichloroacetyl chloride → HCID 20340652, compound

Participants

Reaction Steps

A mixture of 3.24 g of 2-(2,2,2-trifluoroethylamino)-5-nitrobenzophenone and 15 ml. of trichloroacetyl chloride was heated at 100° C. (bath temperature) for 5 hours. The volatiles were removed under reduced pressure. The residue was chromatographed on silica gel using benzene as an eluent to give 2-[N-(2,2,2-trifluoroethyl)trichloroacetamido]-5-nitrobenzophenone as an yellow oil.

Provenance & Evidence