Ethyl diazoacetate → HCID 12389515, compound

Participants

Reaction Steps

A mixture of 60 g of ethyl diazoacetate and 100 g of decene was added drop-by-drop to a stirred suspension of 4 g of anhydrous copper sulfate in 700 g of decene, at 105° C. The addition required 1.5 hours. The mixture was stirred for an additional 2 hours, then filtered, and the filtrate was distilled, to give 1, as a liquid, bp: 107°-110° C. (0.1 Torr.).

Provenance & Evidence