HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chloroform → 1-Hexadecanesulfonyl chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chloroform | HCID 6212 | — |
| Reactant | 4-Chloro-3-nitroaniline | HCID 12477 | — |
| Reactant | 1-Hexadecanesulfonamide, N-(4-chloro-3-nitrophenyl)- | HCID 113045 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | 1-Hexadecanesulfonyl chloride | HCID 96923 | — |
Reaction Steps
Hexadecanesulfonylchloride, which was prepared by the method as described in J. M. Sprague, et al., J. Amer. Chem. Soc., Vol. 59, page 1837 (1937), was reacted with 2-chloro-5-aminonitrobenzene in a chloroform solution in the presence of pyridine to prepare 2-chloro-5-hexadecanesulfonamidonitrobenzene.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04203768 |
| Source dataset | uspto-grants-1980_05 |
| ORD ID | ord-5355f19072274c93ae6b27039e772a72 |
| Source note | uspto-grants-1980_05 |