HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-(((2-Aminoethyl)thio)methyl)-N,N-dimethyl-2-furanmethanamine → N-Cyano-N'-(2-propyn-1-yl)-N"-{2-[(5-dimethylaminomethyl-2-furyl)methylthio]ethyl}guanidine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-(((2-Aminoethyl)thio)methyl)-N,N-dimethyl-2-furanmethanamine | HCID 162203 | — |
| Reactant | Carbamimidothioic acid, N-cyano-N'-2-propynyl-, methyl ester | HCID 2805748 | — |
| Product | N-Cyano-N'-(2-propyn-1-yl)-N"-{2-[(5-dimethylaminomethyl-2-furyl)methylthio]ethyl}guanidine | HCID 136088352 | — |
Reaction Steps
The product of Step A is reacted with about an equimolar amount of 2-[(5-dimethylaminomethyl-2-furyl)methylthio]ethylamine in a non-reactive solvent to give, after workup and chromatography as in Example 3, the title product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04203909 |
| Source dataset | uspto-grants-1980_05 |
| ORD ID | ord-94d2b60317074c9191de57358d65310e |
| Source note | uspto-grants-1980_05 |