HRID1395380

反应详情

EQUATION

反应方程式

HRID 1395380 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

A mixture of 1-nitro-2-methylthio-2-{2-[(5-methylaminomethyl-2-furyl)methylthio]ethylamino}ethylene [prepared according to the procedure described in Belgian Pat. No. 857,388] and propargylamine in acetonitrile is stirred and heated under a positive pressure of nitrogen to give, after workup and chromatography, the title compound.

WORKUP

后处理

  1. customprepared
  2. temperatureheated under a positive pressure of nitrogen
  3. customto give