Dimethyl N-cyanodithioiminocarbonate → HCID 136096282, compound

HRID 1395390Notes

Reaction equation

HRID 1395390 reaction equation
C(N=C(SC)SC)#N.CC1[CH:14]=[C:13]([CH2:15][N:16](C)C)OC=1CSCCN.[C:24]([NH:26][C:27](=[N:30][CH2:31][CH2:32][S:33][CH2:34][C:35]1[O:36][C:37]([CH2:41][N:42]([CH3:44])[CH3:43])=[CH:38][C:39]=1[CH3:40])SC)#[N:25].C(N)C#C>>[C:24]([NH:26][C:27]([NH:16][CH2:15][C:13]#[CH:14])=[N:30][CH2:31][CH2:32][S:33][CH2:34][C:35]1[O:36][C:37]([CH2:41][N:42]([CH3:44])[CH3:43])=[CH:38][C:39]=1[CH3:40])#[N:25]

Participants

5

Reactant 4

HCID 66289Dimethyl N-cyanodithioiminocarbonateHCID 239041PropargylamineHCID 12943529HCID 12943529, compoundHCID 12943531HCID 12943531, compound

Product 1

HCID 136096282HCID 136096282, compound

Procedure

When an alcohol solution of dimethyl cyanodithioimidocarbonate is reacted with 2-[(3-methyl-5-dimethylaminomethyl-2-furyl)methylthio]ethylamine, and the resultant N-cyano-N'-{2-[(3-methyl-5-dimethylaminomethyl-2-furyl)methylthio]ethyl}-S-methylisothiourea is treated with propargylamine according to the general procedure of Example 3, the title compound is produced.

Sources & evidence

ORD record
ord-8d7bdac51a0e4b23bd2cb424144332be
Source dataset
uspto-grants-1980_05
Patent number
US04203909

Reaction notes

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