Diisopropylphosphorohydrazidate → 1-Acetyl-2-Diisopropoxyphosphoryl Hydrazine

HRID 1395392Notes

Reaction equation

HRID 1395392 reaction equation
[C:1](NNP(OCC)(OCC)=O)(=[O:3])[CH3:2].[CH:14]([O:17][P:18]([NH:24][NH2:25])(=[O:23])[O:19][CH:20]([CH3:22])[CH3:21])([CH3:16])[CH3:15]>N1C=CC=CC=1>[C:1]([NH:25][NH:24][P:18]([O:17][CH:14]([CH3:15])[CH3:16])([O:19][CH:20]([CH3:21])[CH3:22])=[O:23])(=[O:3])[CH3:2]

Participants

4

Reactant 2

HCID 237574DiisopropylphosphorohydrazidateHCID 125485571-Acetyl-2-Diethoxyphosphoryl Hydrazine

Product 1

HCID 203392911-Acetyl-2-Diisopropoxyphosphoryl Hydrazine

Reagents, catalysts & solvents 1

HCID 1049PyridineSolvent

Procedure

This compound was prepared in a similar manner to the compound of Example 1, but using diisopropylphosphorohydrazidate instead of diethylphosphorohydrazidate, and pyridine in place of triethylamine. The product distilled at 130°-140° C./0.07 mm.

Workup

  1. distillationThe product distilled at 130°-140° C./0.07 mm

Sources & evidence

ORD record
ord-6b1960ebbf4b49acaa7f3137cfe04fe7
Source dataset
uspto-grants-1980_05
Patent number
US04203932

Reaction notes

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