HRID1395392
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
AUXILIARIES
试剂、催化剂与溶剂
PROCEDURE
实验过程
This compound was prepared in a similar manner to the compound of Example 1, but using diisopropylphosphorohydrazidate instead of diethylphosphorohydrazidate, and pyridine in place of triethylamine. The product distilled at 130°-140° C./0.07 mm.
WORKUP
后处理
- distillationThe product distilled at 130°-140° C./0.07 mm