HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diisopropylphosphorohydrazidate → 1-Acetyl-2-Diisopropoxyphosphoryl Hydrazine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diisopropylphosphorohydrazidate | HCID 237574 | — |
| Reactant | 1-Acetyl-2-Diethoxyphosphoryl Hydrazine | HCID 12548557 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | 1-Acetyl-2-Diisopropoxyphosphoryl Hydrazine | HCID 20339291 | — |
Reaction Steps
This compound was prepared in a similar manner to the compound of Example 1, but using diisopropylphosphorohydrazidate instead of diethylphosphorohydrazidate, and pyridine in place of triethylamine. The product distilled at 130°-140° C./0.07 mm.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04203932 |
| Source dataset | uspto-grants-1980_05 |
| ORD ID | ord-6b1960ebbf4b49acaa7f3137cfe04fe7 |
| Source note | uspto-grants-1980_05 |