HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Bromoethanol → HCID 3051839, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Bromoethanol | HCID 10898 | — |
| Reactant | HCID 22345216 | HCID 22345216 | — |
| Solvent | 1-Butanol | HCID 263 | — |
| Product | HCID 3051839 | HCID 3051839 | — |
Reaction Steps
10 g (0.04 mole) 4-(3-Trifluoromethyl-4-fluorophenyl)piperazine and 7 g (0.056 mole) 2-bromoethanol are heated under reflux for 4 hours in 60 ml n-butanol. The mixture is left to cool, filtered and then recrystallised from ethanol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04203986 |
| Source dataset | uspto-grants-1980_05 |
| ORD ID | ord-50d9b4073e544fca828a272c53607494 |
| Source note | uspto-grants-1980_05 |