HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Anhydride → N-[6-(Dimethylamino)-2-pyridinyl]acetamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Anhydride | HCID 7918 | — |
| Reactant | N,N-Dimethyl-2,6-pyridinediamine | HCID 22287845 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | N-[6-(Dimethylamino)-2-pyridinyl]acetamide | HCID 20339658 | — |
Reaction Steps
Acetylation of 2-amino-6-dimethylaminopyridine from Part A with acetic anhydride in benzene for 2 hours at reflux gives a quantative yield of the title compound. Melting point is 118°-119°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04203988 |
| Source dataset | uspto-grants-1980_05 |
| ORD ID | ord-b32c3fbbd5f0466e87b1ec0c620caa01 |
| Source note | uspto-grants-1980_05 |