HRID1395618

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID10757

2-Chloroacetophenone

C8H7ClO

HCID516872

Potassium thiocyanate

CKNS

PRODUCTS

生成物

HCID219693

Phenacyl thiocyanate

C9H7NOS

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID702

Ethanol

C2H6O

溶剂HCID962

Water

H2O

CONDITIONS

反应条件

温度: 50 °C

PROCEDURE

实验过程

150 g of ω-chloroacetophenone are dissolved at 50° C. in 1000 ml of ethanol, followed by the addition of a solution of 102 g of KSCN in 40 ml of water. After stirring for 10 minutes at 50° C., the ω-thiocyano acetophenone formed is precipitated with water.