Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | 2-Chloroacetophenone | HCID 10757 | — |
| Reactant | Potassium thiocyanate | HCID 516872 | — |
| Solvent | Ethanol | HCID 702 | — |
| Solvent | Water | HCID 962 | — |
| Product | Phenacyl thiocyanate | HCID 219693 | — |
Reaction Steps
150 g of ω-chloroacetophenone are dissolved at 50° C. in 1000 ml of ethanol, followed by the addition of a solution of 102 g of KSCN in 40 ml of water. After stirring for 10 minutes at 50° C., the ω-thiocyano acetophenone formed is precipitated with water.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04204867 |
|---|
| Source dataset | uspto-grants-1980_05 |
|---|
| ORD ID | ord-7b8bd479b84f475ab2cab32ca67c4a53 |
|---|
| Source note | uspto-grants-1980_05 |
|---|
