HuagongsheHuagongshe Chemistry Print Report · For research reference only
Aniline → 2-anilinoacetophenone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Aniline | HCID 6115 | — |
| Reactant | Phenacyl bromide | HCID 6259 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 2-anilinoacetophenone | HCID 1132624 | — |
Reaction Steps
100 g of ω-bromoacetophenone are dissolved in 600 ml of absolute ethanol, followed by the dropwise addition at 20° C. of 100 g of aniline. On completion of the addition, the ω-anilinoacetophenone formed precipitates in crystalline form. Yield: 62 g=59%; m.p: 97°-99° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04204867 |
| Source dataset | uspto-grants-1980_05 |
| ORD ID | ord-a199748a486c4f828cfb82e1f4a92777 |
| Source note | uspto-grants-1980_05 |