Methyl iodide → HCID 20337872, compound

Participants

Reaction Steps

In 10 ml. of acetone was dissolved 0.1 g. of 2-(diphenylmethylene)quinolizidine. After 1.0 ml. of methyl iodide was added to the solution, the mixture was stirred at room temperature of 24 hrs. The precipitated crystals were removed by filtration and recrystallized from methanol to give 0.1 g. of colorless needles having a melting point of 280° to 282° C.(decomposed).

Provenance & Evidence