Methyl iodide → HCID 20337886, compound

Participants

Reaction Steps

In 30 ml. of methanol was dissolved 2.0 g. of 3-diphenylmethylenequinolizidine. After adding 1.5 ml. of methyl iodide to the solution, the mixture was stirred at room temperature for 24 hrs. After completion of the reaction, the solvent was distilled off and the resulting crystals were recrystallized from acetone to obtain 1.6 g. of colorless prisms showing a melting point of 221° to 224° C.

Provenance & Evidence