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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1395657Generated: October 30, 2026

Methyl iodide → HCID 20337878, compound

https://huagongshe.com/reaction/1395657

Reaction equation

Participants

RoleNameHCIDCharge
ReactantMethyl iodideHCID 6328—
ReactantHCID 12519300HCID 12519300—
SolventAcetoneHCID 180—
ProductHCID 20337878HCID 20337878—

Reaction Steps

To a solution of 0.3 g. of 1-(dithien-2-ylmethylene)-quinolizidine in 5 ml. of anhydrous acetone was added 1 ml. of methyl iodide. The mixture was stirred at room temperature for 1 hr. The formed crystals were collected by filtration. By recrystallizing from isopropanol, 0.3 g. of light brown needles having a melting point of 284°-285° C. (decompd.) were obtained.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04205074
Source datasetuspto-grants-1980_05
ORD IDord-f8a38c800e8d458aaee13cbaa961e6cd
Source noteuspto-grants-1980_05