HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → HCID 20337878, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | HCID 12519300 | HCID 12519300 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 20337878 | HCID 20337878 | — |
Reaction Steps
To a solution of 0.3 g. of 1-(dithien-2-ylmethylene)-quinolizidine in 5 ml. of anhydrous acetone was added 1 ml. of methyl iodide. The mixture was stirred at room temperature for 1 hr. The formed crystals were collected by filtration. By recrystallizing from isopropanol, 0.3 g. of light brown needles having a melting point of 284°-285° C. (decompd.) were obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04205074 |
| Source dataset | uspto-grants-1980_05 |
| ORD ID | ord-f8a38c800e8d458aaee13cbaa961e6cd |
| Source note | uspto-grants-1980_05 |