Methyl Bromide → HCID 70596338, compound

Participants

Reaction Steps

In 10 ml. of acetone was dissolved 0.5 g. of 1-diphenylmethyleneindolizidine. To the resulting solution was added 2 ml. of methyl bromide. The mixture was allowed to stand for 30 mins. The crystals obtained after distilling of the solvent were washed with acetone to obtain 540 mg. of colorless plate-like crystals showing a melting point of 210°-211° C. were obtained.

Provenance & Evidence