HuagongsheHuagongshe Chemistry Print Report · For research reference only
Allylamine → HCID 20337912, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Allylamine | HCID 7853 | — |
| Reactant | HCID 20337911 | HCID 20337911 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 20337912 | HCID 20337912 | — |
Reaction Steps
An ethanol solution of 1E and an excess of 2-propenamine was refluxed for 2.5 days. The excess amine and the solvent were evaporated under reduced pressure. The resulting gum was recrystallized from methylene chloride/hexane to give 1, as a white solid, mp: 112° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04205080 |
| Source dataset | uspto-grants-1980_05 |
| ORD ID | ord-1d615ecc0105419eb323e41545e349d2 |
| Source note | uspto-grants-1980_05 |