Allylamine → HCID 20337907, compound

HRID 1395688Notes

Reaction equation

HRID 1395688 reaction equation
[C:1]([NH:4][C:5]1[CH:10]=[CH:9][C:8]([C:11]2[CH:12]=[CH:13][C:14]3[O:18][CH:17]([C:19](OCC)=[O:20])[CH2:16][C:15]=3[CH:24]=2)=[CH:7][CH:6]=1)(=[O:3])[CH3:2].[CH2:25]([NH2:28])[CH:26]=[CH2:27]>C(O)C>[C:1]([NH:4][C:5]1[CH:6]=[CH:7][C:8]([C:11]2[CH:12]=[CH:13][C:14]3[O:18][CH:17]([C:19]([NH:28][CH2:25][CH:26]=[CH2:27])=[O:20])[CH2:16][C:15]=3[CH:24]=2)=[CH:9][CH:10]=1)(=[O:3])[CH3:2]

Participants

4

Reactant 2

HCID 7853AllylamineHCID 20337909HCID 20337909, compound

Product 1

HCID 20337907HCID 20337907, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

20 ml of ethanol was added to a mixture of 1.6 g of 7D and 20 ml of 2-propenylamine. The mixture was stirred for 3 hours at room temperature. The solid which formed was collected, washed with ethanol, then ether and dried under reduced pressure to give 7, mp: 244°-247° C.

Workup

  1. customThe solid which formed
  2. customwas collected
  3. washwashed with ethanol
  4. dry with materialether and dried under reduced pressure
  5. customto give 7, mp: 244°-247° C.

Sources & evidence

ORD record
ord-a8cfa7df2752454781c5cf66e655bb31
Source dataset
uspto-grants-1980_05
Patent number
US04205080

Reaction notes

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