Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
4-[15-(Trifluoromethyl)pentadecylamino]benzoic acid → 4-[15-(Trifluoromethyl)pentadecylamino]benzoyl chloride hydrochloride
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 4-[15-(Trifluoromethyl)pentadecylamino]benzoic acid | HCID 12831610 | — |
| 반응물 | Dimethoxyethane methylene chloride | HCID 86634710 | — |
| 생성물 | 4-[15-(Trifluoromethyl)pentadecylamino]benzoyl chloride hydrochloride | HCID 20549317 | — |
반응 단계
A cold solution of 25 g. of 4-[15-(trifluoromethyl)pentadecylamino]benzoic acid in 500 ml. dimethoxyethane-methylene chloride (4:1) is prepared and dry hydrochloric acid is bubbled through the solution until no more precipitate forms. The solution is treated with 25 ml. thionyl chloride and refluxed until all of the precipitate has dissolved. The solvents are evaporated to yield 4-[15-(trifluoromethyl)pentadecylamino]benzoyl chloride hydrochloride as an orange, semi-crystalline mass.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04205085 |
| 출처 데이터셋 | uspto-grants-1980_05 |
| ORD ID | ord-bfb426177f05433998272a53dc95cc46 |
| 출처 메모 | uspto-grants-1980_05 |