Hydrochloric Acid → HCID 178479232, compound

HRID 1395787Notes

Reaction equation

HRID 1395787 reaction equation
C([NH:4][CH2:5][CH2:6][N:7]1[C:11]([SH:12])=[N:10][N:9]=[N:8]1)(=O)C.[ClH:13]>>[ClH:13].[NH2:4][CH2:5][CH2:6][N:7]1[C:11]([SH:12])=[N:10][N:9]=[N:8]1

Participants

3

Reactant 2

HCID 313Hydrochloric AcidHCID 178474869HCID 178474869, compound

Product 1

HCID 178479232HCID 178479232, compound

Procedure

A mixture of 1-(2-acetamidoethyl)-1H-tetrazole-5-thiol (1.56 g.) in 6 N-hydrochloric acid (20 ml.) was heated under reflux for 2 hours and the resulting solution was evaporated to dryness under reduced pressure. The residue was dried over potassium hydroxide under reduced pressure to give 1-(2-aminoethyl)-1H-tetrazole-5-thiol hydrochloride (1.45 g.), m.p. 190° to 193° C. (dec.).

Workup

  1. temperaturewas heated
  2. temperatureunder reflux for 2 hours
  3. customthe resulting solution was evaporated to dryness under reduced pressure
  4. dry with materialThe residue was dried over potassium hydroxide under reduced pressure

Sources & evidence

ORD record
ord-2871f02e51ad4b7cb2ca95d9281fddea
Source dataset
uspto-grants-1980_05
Patent number
US04205166

Reaction notes

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