HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 10931845, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Morpholine | HCID 8083 | — |
| Reactant | Tetrahydro-4H-pyran-4-one | HCID 121599 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 10931845 | HCID 10931845 | — |
Reaction Steps
650 mg of tetrahydro-4H-pyran-4-one together with 950 mg of morpholine were dissolved in 10 ml of toluene and the mixture was heated under reflux in a light water separator for 5 hours. Subsequently, the mixture was concentrated under reduced pressure, and residue (1.3 g) was used further without further workup.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08901114B2 |
| Source dataset | uspto-grants-2014_12 |
| ORD ID | ord-57ca641536d6442982df03e023b77d34 |
| Source note | uspto-grants-2014_12 |