HuagongsheHuagongshe Chemistry Print Report · For research reference only
Boronic Acid → [3,3'-Bithiophene]-5-carbaldehyde
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Boronic Acid | HCID 61668 | — |
| Reactant | 4-Bromothiophene-2-carbaldehyde | HCID 87792 | — |
| Reactant | Thiophene-3-boronic acid | HCID 581760 | — |
| Product | [3,3'-Bithiophene]-5-carbaldehyde | HCID 16218061 | — |
Reaction Steps
[3,3′-bithiophene]-5-carbaldehyde was prepared using the general boronic acid coupling procedure with 4-bromothiophene-2-carbaldehyde and thiophen-3-ylboronic acid (56 mg, 102 mg theoretical, 54.9%). LC-MS m/z 195 (M+1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08901145B2 |
| Source dataset | uspto-grants-2014_12 |
| ORD ID | ord-fd9ad87ec7a24e0eba456bd77b4da529 |
| Source note | uspto-grants-2014_12 |