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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1397234Generated: November 2, 2026

2-Bromoacetamidopyridine → HCID 24699189, compound

https://huagongshe.com/reaction/1397234

Reaction equation

Participants

RoleNameHCIDCharge
Reactant2-BromoacetamidopyridineHCID 38384—
Reactant2-CyanoethanethioamideHCID 1416277—
ProductHCID 24699189HCID 2469918973%

Reaction Steps

This compound was synthesized from 2-bromo-1-(pyridin-2-yl)ethanone and 2-cyanothioacetamide as described in example 1 step 1 (0.37 g, yield 73%): 1H NMR (400 MHz, CDCl3) δ 8.65 (d, J=5.5 Hz, 1H), 8.15 (m, 2H), 7.84 (t, J=8.4 Hz, 1H), 7.30 (m, 1H), 4.21 (s, 2H). MS (ESI) m/z: Calculated for C10H7N3S: 201.04. found: 202.2 (M+H)+.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08901156B2
Source datasetuspto-grants-2014_12
ORD IDord-028af488c5fc4d82874916dddc5f6e8e
Source noteuspto-grants-2014_12