HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Bromoacetamidopyridine → HCID 24699189, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Bromoacetamidopyridine | HCID 38384 | — |
| Reactant | 2-Cyanoethanethioamide | HCID 1416277 | — |
| Product | HCID 24699189 | HCID 24699189 | 73% |
Reaction Steps
This compound was synthesized from 2-bromo-1-(pyridin-2-yl)ethanone and 2-cyanothioacetamide as described in example 1 step 1 (0.37 g, yield 73%): 1H NMR (400 MHz, CDCl3) δ 8.65 (d, J=5.5 Hz, 1H), 8.15 (m, 2H), 7.84 (t, J=8.4 Hz, 1H), 7.30 (m, 1H), 4.21 (s, 2H). MS (ESI) m/z: Calculated for C10H7N3S: 201.04. found: 202.2 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08901156B2 |
| Source dataset | uspto-grants-2014_12 |
| ORD ID | ord-028af488c5fc4d82874916dddc5f6e8e |
| Source note | uspto-grants-2014_12 |