HRID1397236

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID407031

2-bromo-1-(pyridin-4-yl)ethanone

C7H6BrNO

HCID1416277

Ethanethioamide, 2-cyano-

C3H4N2S

PRODUCTS

生成物

HCID24710447

未命名化合物

收率 46%

PROCEDURE

实验过程

This compound was synthesized from 2-bromo-1-(pyridin-4-yl)ethanone and 2-cyanothioacetamide as described in example 1 step 1 (0.23 g, yield 46%): 1H NMR (300 MHz, MeOD) δ 8.59 (m, 2H), 8.24 (s, 1H), 7.98 (m, 2H), 4.44 (s, 2H). MS (ESI) m/z: Calculated for C10H7N3OS: 201.01. found: 202.2 (M+H)+.