HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Bromo-4'-(trifluoromethyl)acetophenone → HCID 2742458, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Bromo-4'-(trifluoromethyl)acetophenone | HCID 321979 | — |
| Reactant | 2-Cyanoethanethioamide | HCID 1416277 | — |
| Product | HCID 2742458 | HCID 2742458 | 48% |
Reaction Steps
This compound was synthesized from 2-bromo-1-(4-(trifluoromethyl)phenyl)ethanone and 2-cyanothioacetamide as described in example 1 step 1 (2.4 g, 48% yield), and it was carried through without further purification. MS (ESI) m/z: Calculated for C12H7F3N2S: 268.03. found: 269.0 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08901156B2 |
| Source dataset | uspto-grants-2014_12 |
| ORD ID | ord-7e5d1bda92664ea1a5f4accf8ea32e89 |
| Source note | uspto-grants-2014_12 |