Bis(2-bromoethyl) ether → HCID 67324490, compound

HRID 1397353Notes

Reaction equation

HRID 1397353 reaction equation
[C:1]1([C:10]2[CH:15]=[CH:14][CH:13]=[CH:12][CH:11]=2)[CH:6]=[CH:5][CH:4]=[C:3]([CH2:7][C:8]#[N:9])[CH:2]=1.Br[CH2:17][CH2:18][O:19][CH2:20][CH2:21]Br>>[C:1]1([C:10]2[CH:15]=[CH:14][CH:13]=[CH:12][CH:11]=2)[CH:6]=[CH:5][CH:4]=[C:3]([C:7]2([C:8]#[N:9])[CH2:21][CH2:20][O:19][CH2:18][CH2:17]2)[CH:2]=1

Participants

3

Reactant 2

HCID 21521Bis(2-bromoethyl) etherHCID 15364226HCID 15364226, compound

Product 1

HCID 67324490HCID 67324490, compound

Procedure

This compound was synthesized from 2-([1,1′-biphenyl]-3-yl)acetonitrile as described in example 1 step 2 using 2-bromoethyl ether (0.5 g, 73%). 1H NMR (300 MHz, CDCl3) δ 7.72-7.71 (m, 1H), 7.62-7.57 (m, 3H), 7.51-7.45 (m, 4H), 7.42-7.37 (m, 1H), 4.15-4.10 (m, 2H), 3.99-3.91 (m, 2H), 2.28-2.20 (m, 4H).

Sources & evidence

ORD record
ord-1c31bd6985644fa094b6bbe5d531f753
Source dataset
uspto-grants-2014_12
Patent number
US08901156B2

Reaction notes

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