HRID1397381

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID3560503

5-Borononicotinic acid

C6H6BNO4

HCID19971587

1-(5-Bromothiophen-2-yl)-2,2,2-trifluoroethan-1-one

C6H2BrF3OS

PRODUCTS

生成物

结构：O=C(O)c1cncc(-c2ccc(C(=O)C(F)(F)F)s2)c1

HCID67325504

未命名化合物

收率 82%

PROCEDURE

实验过程

This compound was synthesized from 1-(5-bromothiophen-2-yl)-2,2,2-trifluoroethanone and 5-borononicotinic acid as described in example 88 step 3 (470 mg, yield 82%). 1H NMR (300 MHz, DMSO-d6) δ 13.74 (br s, 1H), 9.30-9.29 (s, 1H), 9.11-9.10 (m, 1H), 8.59-8.58 (t, J=2.0 Hz, 1H), 8.20-8.19 (m, 1H), 8.07-8.05 (m, 1H).