Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1398057Generated: November 2, 2026

HCID 86722011, compound → HCID 136253053, compound

https://huagongshe.com/reaction/1398057

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 86722011HCID 86722011—
CatalystPalladiumHCID 23938—
SolventMethanolHCID 887—
ProductHCID 136253053HCID 136253053100%

Reaction Steps

Palladium on carbon catalyst (5%, 400 mg) and 5-(4-(benzyloxy)phenyl)-1-(2-methoxyphenyl)-3-(2,2,6,6-tetramethyltetrahydro-2H-pyran-4-yl)-1H-pyrazole (257.8 mg, 0.52 mmol) were taken in MeOH (10 mL) and stirred under a H2 atmosphere (balloon) for 18 h. The catalyst was removed by filtration and the solvent was removed under vacuum to give 211 mg (100%) of the title compound.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08901314B2
Source datasetuspto-grants-2014_12
ORD IDord-a5abdf9b99e84b73850504ffba7acf12
Source noteuspto-grants-2014_12