HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 117716382, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 6-(4-Nitrophenoxy)hexanoic acid | HCID 22388905 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 117716382 | HCID 117716382 | — |
Reaction Steps
A mixture of 6-(4-nitrophenoxy)-hexanoic acid (20 g), thionyl chloride (40 ml) and dimethylformamide (0.5 ml) was refluxed for 5 hours. Excess thionyl chloride was distilled off under reduced pressure. Dry toluene (20 ml) added and solvent was removed under reduced pressure to obtain 6-(4-nitrophenoxy)-hexanoyl chloride (20 grams) as light yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08901347B1 |
| Source dataset | uspto-grants-2014_12 |
| ORD ID | ord-c94c4f5ed5864f70acdb4e05e49d4f36 |
| Source note | uspto-grants-2014_12 |