HuagongsheHuagongshe Chemistry Print Report · For research reference only
Perbenzoic acid → (2-Ethoxycarbonyloxy-5-octanoylbenzoyl)benzoyl peroxide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Perbenzoic acid | HCID 523077 | — |
| Reactant | 2-Ethoxycarbonyloxy-5-octanoylbenzoyl chloride | HCID 86680240 | — |
| Product | (2-Ethoxycarbonyloxy-5-octanoylbenzoyl)benzoyl peroxide | HCID 53253035 | 26% |
Reaction Steps
In a manner similar to that of Example 1-4, starting with 5.79 g (16.3 mmol) of 2-ethoxycarbonyloxy-5-octanoylbenzoyl chloride and 3.38 g (24.5 mmol) of perbenzoic acid (prepared as described in Example 1-3), 2 g of (2-ethoxycarbonyloxy-5-octanoyl)benzoyl peroxide are obtained in the form of a colourless oil in a yield of 26%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08901357B2 |
| Source dataset | uspto-grants-2014_12 |
| ORD ID | ord-dc16f8289a8f48ac890ba5188e3ab0b3 |
| Source note | uspto-grants-2014_12 |