Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | HCID 16063410 | HCID 16063410 | — |
| Product | HCID 178439571 | HCID 178439571 | — |
Reaction Steps
1-benzyl-4-propyl-1H-1,2,3-triazole prepared above and excess iodomethane were added to a 20 mL vial. The reaction was heated at 40° C. for 3 days. The iodomethane was allowed to evaporate in the hood. The crude product was dissolved with 2 mL CH2Cl2 under reflux. The solution was precipitated into a mixture of acetone, ethyl acetate and hexane and dried in vacuo. The following structure was confirmed:
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US08906135B1 |
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| Source dataset | uspto-grants-2014_12 |
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| ORD ID | ord-0c1fe18526954c2d8f7f6f58e891cd05 |
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| Source note | uspto-grants-2014_12 |
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