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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1399381Generated: October 31, 2026

Methyl iodide → HCID 178439571, compound

https://huagongshe.com/reaction/1399381

Reaction equation

Participants

RoleNameHCIDCharge
ReactantMethyl iodideHCID 6328—
ReactantHCID 16063410HCID 16063410—
ProductHCID 178439571HCID 178439571—

Reaction Conditions

Temperature40 °C

Reaction Steps

1-benzyl-4-propyl-1H-1,2,3-triazole prepared above and excess iodomethane were added to a 20 mL vial. The reaction was heated at 40° C. for 3 days. The iodomethane was allowed to evaporate in the hood. The crude product was dissolved with 2 mL CH2Cl2 under reflux. The solution was precipitated into a mixture of acetone, ethyl acetate and hexane and dried in vacuo. The following structure was confirmed:

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08906135B1
Source datasetuspto-grants-2014_12
ORD IDord-0c1fe18526954c2d8f7f6f58e891cd05
Source noteuspto-grants-2014_12