HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 125482867, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Trimethylsilylacetylene | HCID 66111 | — |
| Reactant | Azidobenzene | HCID 69319 | — |
| Reactant | Sodium Ascorbate | HCID 23667548 | — |
| Catalyst | Copper Sulfate | HCID 24462 | — |
| Solvent | 1-Butanol | HCID 263 | — |
| Product | HCID 125482867 | HCID 125482867 | — |
Reaction Steps
Trimethylsilylacetylene, phenylazide, copper (II) sulfate and sodium (R)-2-((S)-1,2-dihydroxyethyl)-4-hydroxy-5-oxo-2,5-dihydrofuran-3-olate were added to a 1:2 solution of water:butan-1-ol. The reaction was stirred for 4 days and t-butanol and water were removed, producing a 1-phenyl-4-((trimethylsilyl)methyl)-1H-1,2,3-triazole solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08906135B1 |
| Source dataset | uspto-grants-2014_12 |
| ORD ID | ord-6c039788de064fb183691a701ddff963 |
| Source note | uspto-grants-2014_12 |